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Упит dcterms_subject_txt:chemical analysis

753 items

  • Freeze-dried nanocrystal dispersion of novel deuterated pyrazoloquinolinone ligand (DK-I-56-1): Process parameters and lyoprotectant selection through the stability study

    Jelena R. Mitrović, Maja Bjelošević Žiberna, Aleksandar Vukadinović, Daniel E. Knutson, Dishary Sharmin, Aleksandar Kremenović, Pegi Ahlin Grabnar, Odon Planinšek, Dominique Lunter, James M. Cook, Miroslav M. Savić, Snežana D. Savić (2023)
    Recently, nanocrystal dispersions have been considered as a promising formulation strategy to improve the bioavailability of the deuterated pyrazoloquinolinone ligand DK-I-56-1 (7‑methoxy-2-(4‑methoxy-d3-phenyl)-2,5-dihydro-3H-pyrazolo[4,3-c]quinolin-3-one). In the current study, the freeze-drying process (formulation and process parameters) was investigated to improve the storage stability of the previously developed formulation. Different combinations of lyoprotectant (sucrose or trehalose) and bulking agent (mannitol) were varied while formulations were freeze-dried under two conditions (primary drying at -10 or -45 °C). The obtained lyophilizates were characterized in terms ...
    Pharmaceutical Science
    ... mean + standard deviation. Statistical analysis included Student t-test (for two sets of results) or one-way ANOVA (for three sets of results) with Tukey HSD as a post hoc test. P values < 0.05 were considered as statistically significant. Statistical analysis was done using IBM SPSS Statistics ...
    ... extend shelf-life more than threefold compared to the liquid state formulation published in Mitrović et al. (2020). 3.3. Physical state analysis Analysis of the physical state of the freeze-dried formulations included differential scanning calorimetry (DSC) and X-ray powder diffraction (XRPD) ...
    ... et al., 2014). Informa- tion about hydrogen bonding can be inferred from analysis of the po- sition and width of the OH-stretching band in the FT-IR spectrum (Sritham and Gunasekaran, 2017). In this study, the analysis included the interpretation of the transmission spectra of bulk excipients ...

  • Long-term rockslope monitoring and rockfall prediction

    Miloš Marjanović, Biljana Abolmasov, Marko Pejić, Jelka Krušić (2021)

  • Prezentacija projekta "Zaštita ležišta mineralnih sirovina kao osnova sigurnog snabdevanja mineralnim sirovinama u Evropi (safemin4europe)

    Vladimir Simić, Rade Jelenković, Dragana Životić, Zoran Miladinović, Stefan Petrović, Marija Petrović (2022)
    Harmonični ekonomski razvoj svake zemlje u velikoj meri zavisi od dostupnosti sirovina, naročito mineralnih sirovina. Obezbeđivanje njihove dovoljne količine na tržištu (ponude) je od vitalnog značaja za funkcionisanje različitih industrijskih grana koje proizvode različitu robu i opremu neophodnu za ispunjavanje životnih potreba stanovništva kao i za efikasnu poljoprivredu. Mineralne sirovine su neophodne za podršku ekonomskim aktivnostima na lokalnom, regionalnom, nacionalnom i međunarodnom nivou. Ovo su, istorijski, prve sirovine koje su počele da se koriste iz domaćih izvora, i u ...
    ležišta mineralnih sirovina, valorizacija, zaštićena područja, socijalni aspekti

  • Komparacija metoda XRF i ICP-MS na uzorcima uglja i produkata sagorevanja

    Branko Kostić, Dejan Prelević, Sabina Kovač, Ksenija Eraković, Dragana Životić (2022)
    Ugljevi niskog ranga – ligniti u Republici Srbiji predstavljaju glavnu energetsku sirovinu koja se koristi za proizvodnju električne energije. Rudarstvo u Srbiji doprinosi bruto dodatoj vrednosti sa 1,8% (2020; https://publikacije.stat.gov.rs/). Sagorevanjem ugljeva niskog ranga u termoelektranama generišu se velike količine elektrofilterskog pepela i pepela, koje često predstavljaju jedan od izvora zagađenja životne sredine usled sadržaja toksičnih elemenata. Dalja upotreba produkata sagorevanja zavisi od njihovog sastava i sadržaja toksičnih mikroelemenata. Svakodnevno sagorevanje lignita u termoelektranama uslovljava konstantan monitoring potencijalno toksičnih ...
    ugalj, produkti sagorevanja, XRF, ICP-MS

  • Geotehnički efekti razaranja komunalnog otpada različitim postupcima zbijanja

    Jovana M. Janković Pantić (2022)
    Odlaganje otpada na komunalne deponije predstavlja osnovni način zbrinjavanja otpada u Srbiji. Kako bi se prostor za deponovanje materijala racionalno koristio potrebno ga je svakodnevno zbijati sa unapred definisanom količinom vode koja se dodaje. Dobro zbijeni komunalni otpad zauzima manju zapreminu i omogućuje sigurnije skladištenje, pa je korisno prethodno laboratorijski odrediti parametre zbijanja: maksimalnu suvu zapreminsku težinu (dmax) i optimalnu vlažnost (wopt). U Srbiji do sada nisu određivani parametri zbijanja, dok je u svetu primenjivana standardna metoda (Proktorov opit) ...
    komunalna deponija, zbijanje, Proktorov opit, malj sa šiljcima, koeficijent razaranja

  • Assessments of effects of implementation of strategic plans for development of Belgrade District heating system

    Dejan Ivezić, Marija Živković, Aleksandar Madžarević, Miodrag Grujić (2020)
    The district heating system (DHS) is one of the key elements of the Belgrade energy system. Overview of the current state and basic characteristics of the DHS are presented in this paper. The focus is on the planned development of DHS and on the analyses of effects of realization of measures and projects defined by strategic documents related to DHS which are adopted by city authorities (Development Strategy of DHS and Strategy of Belgrade Development). Two exploratory scenarios were ...
    Daljinsko grejanje, LEAP, Primarni energetski faktor, Uvozna zavisnost, CO2 emisija

  • Determination of Mechanical Properties of Altered Dacite by Laboratory Methods

    Veljko Rupar, Vladimir Čebašek, Vladimir Milisavljević, Dejan Stevanović, Nikola Živanović (2021)
    This paper presents a methodology for determining the uniaxial and triaxial compressive strength of heterogeneous material composed of dacite (D) and altered dacite (AD). A zone of gradual transition from altered dacite to dacite was observed in the rock mass. The mechanical properties of the rock material in that zone were determined by laboratory tests of composite samples that consisted of rock material discs. However, the functional dependence on the strength parameter alteration of the rock material (UCS, intact ...
    Geology, Geotechnical Engineering, Engineering Geology
    ... for different participation of AD. Minerals 2021, 11, 813 12 of 19 Also, the analysis included relationships between shear and normal stresses that were constructed based on the Mohr circles of stress. This analysis determined the envelopes for all analyzed participation of altered dacite, which ...
    ... strength σci on the participation of altered dacite (AD%) based on the analysis of laboratory test results is shown in Figure 13. An exponential and linear function Minerals 2021, 11, 813 13 of 19 approximates the analysis results shown in the diagram (Figure 13), and the dependence σci TX—AD% ...
    ... assessing rock mass input parameters necessary for geotechnical stability analysis and detailed design solutions. Author Contributions: Conceptualization, V.R.; methodology, V.R. and V.Č.; validation, V.M., D.S. and N.Ž.; formal analysis, V.R. and V.Č.; investigation, V.R., V.Č., V.M., D.S. and N.Ž.; resources ...

  • The external aggregation Newton's method for solving nonlinear equations and applications

    Marija Paunović, Dejan Ćebić, Nebojša Ralević (2020)
    Њутнов метод, агрегациона функција, ред конвергенције

  • Fuzzy Model for Risk Assessment of Machinery Failures

    Dejan V. Petrović, Miloš Tanasijević, Saša Stojadinović, Jelena Ivaz, Pavle Stojković (2020)
    The main goal of this research was the development of an algorithm for the implementation of negative risk parameters in a synthesis model for a risk level assessment for a specific machine used in the mining industry. Fuzzy sets and fuzzy logic theory, in combination with statistical methods, were applied to analyze the time picture state of the observed machine. Fuzzy logic is presented through fuzzy proposition and a fuzzy composition module. Using these tools, the symmetric position of the ...
    fazi teorija, rizik, otkaz rudarskih mašina
    ... n and a Failure Mode and Effects Analysis (FMEA). RPN methodology is a technique for analyzing the risk associated with any potential problems identified during an FMEA. However, there is a great deal of debate among FMEA practitioners as to the correct analysis procedure, and some analyses may include ...
    ... Z. Criticality analysis of petrochemical assets using risk based maintenance and the fuzzy inference system. Process Saf. Environ. 2019, 121, 312–325. [CrossRef] 17. Chandima Ratnayakea, R.M.; Antosz, K. Development of a Risk Matrix and extending the risk-based maintenance analysis with fuzzy logic ...
    ... H.-C.; Liu, L.; Liu, N. Risk evaluation approaches in failure mode and effects analysis: A literature review. Expert Syst. Appl. 2013, 40, 828–838. [CrossRef] 23. Kahneman, D.; Tversky, A. Prospect theory: An analysis of decision under risk. In Handbook of the Fundamentals of Financial Decision Making: ...

  • Geologic Information System of Serbia

    Branislav Blagojević, Branislav Trivić, Ranka Stanković, Nenad Banjac, Olivera Kitanović (2011)
    Geologic information system of Serbia (GeolISS) represents repository for digital archiving, query, retrieving, analysis and geologic data visualization. The GeolISS is implemented through ESRI ArcGIS technology, and is designed to operate as a personal geodatabase (MS Jet 4.0 Engine) and SDE enterprise geodatabase in MS SQL Server. The objective of GeolISS implementation is integration of existing geologic archives, data from published maps at different scales, newly acquired field data, as well as Web publishing of geologic information. Physical implementation ...
    Geologic information system, Conceptual model, Logical model, Implementation, Geodatabase
    ... Implementation, Geodatabase. Geologic information system of Serbia (GeolISS) represents repository for digital archiving, query, retrieving, analysis and geologic data visualization. The GeolISS is implemented through ESRI ArcGIS technology, and is designed to operate as a personal geodatabase ...

  • Korelacija magnetnog susceptibiliteta i sadržaja metala u flotacijskom jalovištu

    Filip Abramović, Vesna Cvetkov, Aco Ilić, Dragana Životić (2022)
    Procena metala u rudama, jalovištu i zemljištu se tradicionalno određuje hemijskim metodama kao što su Rengen fluorescentna analiza (XRF), Instrumentalna neutronska aktivaciona analiza (INAA) i Masena spektrometrija induktivno spregnute plazme (ICP-MS). Neke od pomenutih metoda su veoma zahtevne i skupe, te se nametnula potreba ka traženju jeftinijeg alata za brzu procenu prisustva pojedinih metala. Tokom poslednjih nekoliko decenija, mnoge studije su pokazale da su magnetna merenja dovoljno osetljiva da detektuju magnetni signal feromagnetnih materijala, a samim tim i metala ...
    flotacijsko jalovište, makroelementi, magnetna merenja

  • Increasing the Local Road Network Resilience from Natural Hazards in Municipalities in Serbia

    Biljana Abolmasov, Miloš Marjanović, Ranka Stanković, Uroš Đurić, Nikola Vulović (2024)
    lokalni putevi, prirodni hazardi, otpornost na klimatske promene, MaPLoRds

  • Evidence for Ladinian (Middle Triassic) platform progradation in the Gyulakeszi area, Tapolca Basin, Western Hungary: Microfacies Analysis and Biostratigraphy

    Zsolt Robert Nagy, Nevenka Đerić, Sándor Kovács, Anna Oravecz-Scheffer, Felicitász Velledits, Olga Piros, Gabor Csillag (2014)
    anizik, ladin, karbonati, litostratigrafija, biostratigrafija, konodonti, radiolarije, dijageneza
    ... the study area (Nagy et al. 1999). 168 Nagy Z.R. & al. Fels6ors Basin Szenitkiraly- szabadja Platform i Microfacies Analysis Ammonite Thin-section analysis has Zonel/Subzone o M been conducted in order to characterize the microfacies of the lower (MF1) and upper unit [-i .9 ...
    ... 2023-11-06 11:13:48 Evidence for Ladinian (Middle Triassic) platform progradation in the Gyulakeszi area, Tapolca Basin, Western Hungary: Microfacies Analysis and Biostratigraphy Zsolt Robert Nagy, Nevenka Đerić, Sándor Kovács, Anna Oravecz-Scheffer, Felicitász Velledits, Olga Piros, Gabor Csillag Дигитални ...
    ... Београду [ДР РГФ] Evidence for Ladinian (Middle Triassic) platform progradation in the Gyulakeszi area, Tapolca Basin, Western Hungary: Microfacies Analysis and Biostratigraphy | Zsolt Robert Nagy, Nevenka Đerić, Sándor Kovács, Anna Oravecz-Scheffer, Felicitász Velledits, Olga Piros, Gabor Csillag | Rivista ...

  • Tectonic evolution of the Circum-Moesian orocline of the Carpatho-Balkanides: Paleomagnetic constraints

    Emő Márton, Vesna Cvetkov, Miodrag Banješević, Gábor Imre, Aleksandar Pačevski (2024)
    Apuseni-Banat-Timok-Srednogorie belt, danubicum, paleomagnetism, oroclinal bending

  • Application of VIКOR method in the selection of an optimal splution of excavation “Borska Reka” ore deposit

    Sanja Bajić, Dragoljub Bajić, Branko Glušćević, Radmila Gaćina (2023)

  • Replica of the “Great Triangle Gold Nugget” Belonging to Belgrade University Collection, Gilded or Not?

    Alena Zdravković, Maja Milošević, Ivana Jelić (2021)
    ... (Oxford Instruments). The small amount of the skim was gently removed from the surface and glued onto a graphite strip, without covering. Chemical analysis was performed on unpolished pieces, using the EDS detector and the internal standards. Historic background The gold nugget was mined ...
    ... the gold colour and shine remained the same, did not darken by the time it was assumed that the model is gilded. Material and method Chemical composition of the gypsum model surface was carried out in the Laboratory for SEM, Faculty of Mining and Geology, University of Belgrade, using ...
    ... number of the replica made, and the type and manner of material that was used for covering. Result and conclusion The data obtained by EDS analysis show that the gypsum model is covered with gold leaf, which was expected according to the macroscopic characteristic of the object. How many ...

  • Cultural Heritage and Protection of Hand-Wheeled Pottery Manufacture in Western Serbia: Characteristics of Zlakusa Pottery Based on Sem-Eds and Optical Microscopy

    Milošević Maja, Zdravković Alena, Đordjević Biljana, Jelić Ivana (2021)
    ... was fabricated. By the size and orientation of the pores, it is evident that the pot was manufactured by the application of a mould. SEM-EDS analysis was performed on the inner parts of the walls of the investigated samples and their surface area. When samples are compared slight difference ...
    ... groundmass and pores have a directional appearance, consistent with previous observations, and a slightly higher amount of calcite grains. EDS analysis gives clear differences in the chemistry of the samples. Sample 1 has a higher content of most investigated elements when compared to sample ...

  • On the optimality of some multi-point methods for finding multiple roots of nonlinear equation

    Ralević Nebojša, Ćebić Dejan (2016)

  • Late and post-collisional tectonic evolution of the Adria-Europe suture in the Vardar Zone

    Emő Márton, Marinko Toljić, Vesna Cvetkov (2022)
    The Vardar Zone is a product of the Triassic-Jurassic opening of the Neotethys, Jurassic obduction, Late Cretaceous/Paleogene consumption of the oceanic crust and continental collision. During the last process, the Eastern Vardar Zone was thrust over the Central and eventually both onto the Western Vardar Zone. The present paleomagnetic and structural study provided new results from the first two zones in the Belgrade area. The younger set of data, together with published ones from the third zone, provide firm ...
    Adria–Europe suture, Vardar Zone, Paleomagnetism, Thrusting, Vertical axis rotation

  • Landslide Umka-the first automated monitoring project in Serbia

    Abolmasov Biljana, Milenković Svetozar, Jelisavac Branko, Vujanic Vladeta (2012)