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Упит dcterms_subject_txt:X-ray diffraction

101 items

  • Kristalografsko proučavanje strukturne desimetrizacije granata grosularsko-andraditske izomorfne serije

    Pavle I. Tančić (2016-09-21)
    U ovoj Doktorskoj disertaciji proučavano je pet različitih zona makroskopski zonarnog grandita sa lokaliteta Meka Presedla (Kopaonik, Srbija). Pomoću hemijske i elektronske analize mikroprobe preračunati su relativno visoko homogeni sastavi zona, t.j.: Grs64±1Adr36±1Sps2 (A), Grs62±1Adr38±1Sps2 (B), Grs59±2Adr40±2Sps2 (C), Grs58±2Adr41±2Sps2 (D) i Grs58±1Adr41±1Sps2 (E). Glavne promene u sastavima izražene formulom: Ca2,93-2,97Mn0,05-0,06Mg0,00-0,01Al1,14-1,26Fe3+0,72-0,83Ti0,00-0,02Si2,97-3,02O12 ukazuju da je jedina značajnija varijacija ustanovljena samo kod Al-Fe3+ raspodela u oktaedarskom položaju. Ovakav hemijski sastav je potvrđen i sa matematičkim proračunima iz IC i Raman analiza. Urađena ...
    Macroscopically zoned grandite, chemical analysis, electron microprobe analysis, Raman, Rietveld, structure, dissymmetrization, space group

  • Atmospheric exposure vs burying: influences on damage intensity of built-in kersantite in the monument of the Small Staircase (Belgrade, Serbia)

    Nevenka Novaković, Predrag Dabić, Vesna Matović (2023)
    Proučavan je efekat „zatrpanog kamena“ na intenzitet procesa degradacije prisutnih na kersantitu koji je ugrađen u spomenik Malo stepenište. Istraživanja su vršena na uzorcima stene iz kamenoloma i na oštećenim kamenim blokovima ugrađenim u spomenik. Dok su neki delovi stepeništa bili pod zemljom 90 godina, većina kamenih elemenata je bila izložena različitim uslovima sredine i antropogenim uticajima. Urađeno je detaljno mapiranje trenutnog stanja spomenika kako bi se istražio uticaj “zatrpavanja” i kompleksne geometrije spomenika na tip propadanja i variranje ...
    Raspadanje, Indeks oštećenja, Zatrpavanje, Fizička svojstva, Kersantit

  • Kristalne strukture Cs2HoSi4O10F i Cs2TmSi4O10F

    Predrag Dabić, Sabina Kovač, Aleksandar Kremenović (2021)
    ... using REE2O3 (REE = Ho, Tm), SiO2 and CsF as starting materials. The crystal structures of both compounds were determined by single-crystal X-ray diffraction analysis. They represent mutually isostructural compounds which crystallize in the orthorhombic space group Pnma with following unit cell p ...

  • Freeze-dried nanocrystal dispersion of novel deuterated pyrazoloquinolinone ligand (DK-I-56-1): Process parameters and lyoprotectant selection through the stability study

    Jelena R. Mitrović, Maja Bjelošević Žiberna, Aleksandar Vukadinović, Daniel E. Knutson, Dishary Sharmin, Aleksandar Kremenović, Pegi Ahlin Grabnar, Odon Planinšek, Dominique Lunter, James M. Cook, Miroslav M. Savić, Snežana D. Savić (2023)
    Recently, nanocrystal dispersions have been considered as a promising formulation strategy to improve the bioavailability of the deuterated pyrazoloquinolinone ligand DK-I-56-1 (7‑methoxy-2-(4‑methoxy-d3-phenyl)-2,5-dihydro-3H-pyrazolo[4,3-c]quinolin-3-one). In the current study, the freeze-drying process (formulation and process parameters) was investigated to improve the storage stability of the previously developed formulation. Different combinations of lyoprotectant (sucrose or trehalose) and bulking agent (mannitol) were varied while formulations were freeze-dried under two conditions (primary drying at -10 or -45 °C). The obtained lyophilizates were characterized in terms ...
    Pharmaceutical Science
    ... Journal of Pharmaceutical Sciences 189 (2023) 106557 2.6. X-ray powder diffraction (XRPD) The physical state of the freeze-dried samples was analyzed by X-ray powder diffraction (XRPD). The analysis was performed on a Rigaku Smartlab X-ray diffractometer in a 0-0 geometry using the D/teX Ultra ...
    ... measuring particle size and calculating redispersibility index, as well as by solid-state analysis (by differential scanning calorimetry and X-ray powder diffraction) and visualization of morphology (by scanning electron microscopy and polarized light microscopy). Finally, the extent of interactions ...
    ... a low background single crystal silicon sample holder to minimize background. Results were analyzed using PDXL2 (v. 2.8.30) integrated X-ray powder diffraction software. 2.7. Scanning electron microscopy (SEM) The morphology of the lyophilzates was analyzed by scanning elec- tron microscopy ...

  • Preparation, synthesis and characterization of nanometric Ca0.9Er0.1MnO3

    Tijana B. Vlašković, Bojana Laban, Maja Milošević, Maria Čebela, Vladimir Dodevski, Milena Rosić (2023)
    ... period of 15 min. The effects of calcination were characterized through different experimental techniques (differential thermal analysis (DTA), X-ray diffraction (KRD), Fourier transform infrared spectroscopy (FTIR), Field emission scanning eclectron microscopy (FESEM), and inductively coupled plasma ...
    ... perovskite: sucrose CoH>»O,,, Which has a dual role (complexant and fuel), and metal nitrates were used as oxidants - calcium nitrate tetrahydrate Ca(NOs),x*4H,O, manganese(II) nitrate hydrate Mn(NOyx)xH,O, erbium(III) nitrate pentahydrate Er(NOs)sx5H,O. Nanopowder was prepared by combining metal nitrates ...

  • Understanding the effect of synthesis and sintering temperature on the functional properties of barium titanate/cobalt ferrite composites

    Marija Šuljagić, Aleksandar Kremenović, Ivan Petronijević, Adis Džunuzović, Miljana Mirković, Vladimir Pavlović, Ljubica Anđelković (2023)
    To investigate the effect of synthesis procedure and sintering temperature on the functional properties of perovskite/spinel ceramics, BaTiO3/CoFe2O4 composites were prepared by thermal decomposition, coprecipitation, and microemulsion method, and sintered at 1150°C and 1300°C. The phase composition and morphology of as-prepared powders as well as sintered ceramics were thoroughly examined by X-ray powder diffraction (XRPD) and scanning electron microscopy (SEM) coupled with electron dispersive spectroscopy (EDS). The dielectric and ferroelectric measurements were performed in detail. Generally, the ...
    Perovskite/spinel ceramics, Multiferroic, Sintering, Influence of synthesis method

  • Agates of the Lece Volcanic Complex (Serbia): Mineralogical and Geochemical Characteristics

    Zoran Miladinović, Vladimir Simić, Nenad Nikolić, Nataša Jović Orsini, Milena Rosić (2024)
    Agate veins and nodules occur in the Lece Volcanic Complex (Oligocene-Miocene) situated in the south of Serbia and occupying an area of 700 km2. This volcanic complex is composed predominantly of andesites, with sporadic occurrences of andesite-basalts, dacites and latites, and features agate formations that have been very little investigated. This study focuses on five selected agate occurrences within the Lece Volcanic Complex, employing optical microscopy, scanning electron microscopy (SEM), X-ray powder diffraction analysis, inductively coupled plasma mass spectrometry ...
    Lecki vulkanski kompleks, andeyit, kalcedon, kvarc, opal-CT, mikrostruktura, organska materija

  • Synthesis and characterization of nanostructured Ca0.9Er0.1MnO3

    Tijana B. Vlašković, Bojana Laban, Maja Milošević, Maria Čebela, Vladimir Dodevski, Milena Rosić (2023)
    ... range of 800-1000 *C for 15min. Particle size, lattice parameters, structural changes, and specific surface area were investigated. DTA, X-ray diffraction (XRD), FTIR, and Field emission scanning electron microscopy (SEM) were used to characterize the synthesized samples at room temperature. ...

  • Examination and characterization of nanostructured Co0.9Ho0.1MoO4

    Милена Росић, Маја Милошевић, Мариа Чебела, Владимир Додевски, Весна Лојпур, Марија Васић, Александра Зарубица (2023)
    ... proven to be a promising method that achieves control of stoichiometry, homogeneity, and purity. The synthesized samples were examined by DTA, X-ray diffraction (XRD), Fourier transform infrared (FT-IR) spectra, Spectroscopy, Field emission scanning electron microscopy (FESEM), and nitrogen adsorption ...

  • Polyhedral characteristics of the cosalite-type crystal structures

    Sabina Kovač, Predrag Dabić, Aleksandar Kremenović, Aleksandar Pačevski, Ljiljana Karanović, Marko V. Rodić, Martina Tribus (2019)
    kristalna struktura, kozalit, poliedarske karakteristike

  • Mikroorganizmi - biohidrogeološki indikatori odabranih pojava mineralnih voda Srbije

    Vladimir Šaraba (2021)
    Sa namerom definisanja hidrogeološke uloge i značaja mikrobiološkog diverziteta odabranih pojava mineralnih voda Srbije, primenom sistema biodetektora, dokazano je prisustvo gvožđevitih, sulfato-redukujućih, sluz-produkujućih, heterotrofnih aerobnih i denitrifikacionih bakterija, na osnovu čega je proračunat rizik od razvoja procesa biokorozije i biohemijske inkrustacije, te zdravstveni rizik. Uz procenu rizika, izvedene su analize skenirajuće elektronske mikroskopije biofilmova i hidrogeohemijsko modeliranje, te makroskopska, otpička i difrakciona ispitivanja naslaga inkrustacije, dok je fizičko-hemijskim analizama utvrđena vrednost ukupne mineralizacije iznad 1 g/L, kao i povišeni ...
    biohidrogeologija, SEM analize, makroskopska i optička ispitivanja, rendgenska difrakcija praha, hidrogeohemijsko modeliranje, BART analize, metabarkoding analize mikrobioma, fizičko-hemijske analize, starenje bunara (biokorozija, biohemijska inkrustacija i biozarastanje), zdravstveni rizik
    ... ogy in the standard hydrogeological research methodology. Keywords: biohydrogeology, SEM analyses, macroscopic and optical assessment, X-ray powder diffraction, hydrogeochemical modelling, BART analyses, metabarcoding of microbiomes, physical and chemical analyses, well aging (biocorrosion, biochemical ...
    ... okruga i njihov uticaj na regionalni razvoj. Doktorska disertacija. Niš: Univerzitet u Nišu, Prirodno-matematički fakultet. Su, X. L., Tian, Q., Zhang, J., Yuan, X. Z., Shi, X. S., Guo, R. B., & Qiu, Y. L. (2014). Acetobacteroides hydrogenigenes gen. nov., sp. nov., an anaerobic hydrogen-producing bacterium ...
    ... health risks were assessed. The research included scanning electron microscopy of biofilms, hydrogeochemical modelling and macroscopic, optical and diffraction examination of the encrustations. Physical and chemical analyses indicated total dissolved salts of more than 1 g/L and elevated concentrations ...

  • Mineralogical and physicochemical characterization of bentonite clay from Svrljig, Serbia

    Maja Milošević, Bojan Kostić (2022)
    ... 3420 cm–1, 1632 cm–1 and 1018 cm–1. The peaks at 1444 cm–1 and 873 cm–1 correspond to carbonate minerals, although in a very small quantity. X-ray diffraction indicates that the bentonite sample is a mixture of montmorillonite as major component, identified by d001 basal spacing value of 15.11 Å at ...
    ... determined by chemical analysis, infrared spectrophotom- etry (Milošević and Logar, 2014; Milošević, 2011), differential thermal analysis (DTA) and X-ray diffrac- tion (powder, oriented, saturated and heated). The physical properties were determined by granulometry (pipette method), cation exchange capacity ...

  • Photocatalytic Activity of the V2O5 Catalyst toward Selected Pharmaceuticals and Their Mixture: Influence of the Molecular Structure on the Efficiency of the Process

    Sanja J. Armaković, Aleksandra Jovanoski Kostić, Andrijana Bilić, Maria M. Savanović, Nataša Tomić, Aleksandar Kremenović, Maja Šćepanović, Mirjana Grujić-Brojčin, Jovana Ćirković, Stevan Armaković (2023)
    Due to the inability of conventional wastewater treatment procedures to remove organic pharmaceutical pollutants, active pharmaceutical components remain in wastewater and even reach tap water. In terms of pharmaceutical pollutants, the scientific community focuses on -blockers due to their extensive (over)usage and moderately high solubility. In this study, the photocatalytic activity of V2O5 was investigated through the degradation of nadolol (NAD), pindolol (PIN), metoprolol (MET), and their mixture under ultraviolet (UV) irradiation in water. For the preparation of V2O5, facile ...
    DFT analysis, metoprolol, nadolol, nanomaterial characterization, photocatalysis, pindolol, β-blocker
    ... scanning, electron microscopy (SEM), X-ray, and Raman spectroscopy. SEM micrographs showed hexagonal-shaped platelets with well- defined morphology of materials with diameters in the range of 10–65 ım and thickness of around a few microns. X-ray diffraction identified only one crystalline phase ...
    ... B-blockers (MET, NAD, and PIN) separately and in a mixture. Several methods of characterization, such as X-ray powder diffraction (KRPD), scanning electron microscopy (SEM), energy-dispersive X-ray spectroscopy (EDS), Brunauer-Emmett-Teller (BET) measurements, Fourier transform infrared (FTIR) and ...
    ... sample was annealed at 500 ?C for 2 h in air. 3.3. Characterization The catalyst was investigated by X-ray powder diffraction (XKRPD). Measurements were conducted on a Rigaku Smartlab X-ray diffractometer in 0-0 geometry (the sample in horizontal position) in part focusing on Bragg-Brentano geometry ...

  • Mineralogical analysis of a clay body from Zlakusa, Serbia, used in the manufacture of traditional pottery

    Maja Milošević, Biljana Đorđević, Mihovil Logar (2020)
    калцит, сирова глина, традиционална керамика, Злакуса
    ... for pottery production in Zlakusa (western Serbia). Particle-size distribution, plasticity, X-ray fluorescence spectroscopy, X-ray powder diffraction, scanning electron microscopy/energy-disper- sive X-ray spectrometry and differential thermal analysis techniques were applied. The mineral phases identified ...
    ... application; and the final clay body (ClIBd) after mixing the CIMx with the CC in the desired ratio. Methods The X-ray powder diffraction (XRPD) data were collected on a Rigaku SmartLab X-ray powder diffractometer using Bragg- Brentano geometry and Cu-Ko. radiation in the scan range of 3-70%0 with a ...
    ... mineral phases were identified using the Rigaku PDXL software and the PDF-2 database (International Centre for Diffraction Data). The chemical com- position was determined by X-ray fluorescence (XRF) spectros- copy using a PANalytical MiniPal 4 XREF spectrometer equipped with a high-resolution ...

  • BaTiO3/NixZn1−xFe2O4 (x = 0, 0.5, 1) Composites Synthesized by Thermal Decomposition: Magnetic, Dielectric and Ferroelectric Properties

    Marija Šuljagić, Ivan Petronijević, Miljana M. Mirković, Aleksandar Kremenović, Adis Džunuzović, Vladimir B. Pavlović, Aleksandra Kalezić-Glišović, Ljubica Andjelković (2023)
    To investigate the influence of spinel structure and sintering temperature on the functional properties of BaTiO3/NixZn1−xFe2O4 (x = 0, 0.5, 1), NiFe2O4, ZnFe2O4, and Ni0.5Zn0.5Fe2O4 were in situ prepared by thermal decomposition onto BaTiO3 surface from acetylacetonate precursors. As-prepared powders were additionally sintered at 1150 °C and 1300 °C. X-ray powder diffraction (XRPD) and scanning electron microscopy (SEM) coupled with electron dispersive spectroscopy (EDS) were used for the detailed examination of phase composition and morphology. The magnetic, dielectric, and ...
    ferroelectric, dielectric properties, magnetic properties, titanate/ferrite composites, phase composition
    ... BaTiOys /Ni„Zni _ „Fe>Ou (x = 0, 0.5, 1), NiFe)Oa, ZnFe>Oxu, and Nip,5Zno sFe>»Oa were in situ prepared by thermal decomposition onto BaTiOy surface from acetylacetonate precursors. As-prepared powders were additionally sintered at 1150 "C and 1300 "C. X-ray powder diffraction (XRPD) and scanning, ...
    ... to room temperature. 3.2. Characterization X-ray powder diffraction (XKRPD) patterns were collected using, Ultima IV Rigaku diffractometer with CuK , radiation (U = 40.0 kV, I = 40.0 mA) equipped with D/TeX Ultra high—speed detector. The diffraction angle range was 10-80* 20 with a step of 0.02" ...
    ... composition of the synthesized materials, as well as, phase abundances are calculated by the RIR method incorporated in PDXL2 integrated X-ray powder diffraction software (Version 2.8.30; Rigaku Corporation, Tokyo, Japan). The morphology and composition of the prepared composites were determined by ...

  • Synthesis, characterization and photocatalytic examination of Co0.9Ho0.1MoO4 nanopowders

    Milena Rosić, Maja Milošević, Maria Čebela, Vladimir Dodevski, Vesna Lojpur, Radomir Ljupković, Aleksandra Zarubica (2023)
    ... Serbia CooSlHop,MoO, nanopowders were obtained by applying glycine nitrate procedure (GNP). The synthesized samples were investigated by DTA, X-ray diffraction (KRD), Fourier transform infrared (FT-IR) spectra, Spectroscopy, Field emission scanning electron microscopy (FESEM), and nitrogen adsorption ...

  • Mineralogical study of clays from Dobrodo, Serbia, for use in ceramics

    Maja Milošević, Predrag Dabić, Sabina Kovač, Lazar Kaluđerović, Mihovil Logar (2019)
    keramika, glina, Dobrodo, mineralogija, sirovina, Srbija

  • Hydrothermal Synthesized and Alkaline Activated Carbons Prepared from Glucose and Fructose—Detailed Characterization and Testing in Heavy Metals and Methylene Blue Removal

    Sanja Krstić, Milan Kragović, Maja Pagnacco, Vladimir Dodevski, Branka Kaluđerović, Miloš Momčilović, Ivica Ristović, Marija Stojmenović (2018)
    glukoza, fruktoza, аktivni ugalj, hidrotermalni tretman, aktivacija hidroksida, teški metali, metilen plavo
    ... LiOH) by hydrothermal treatment (HTC) treatment. After preparation, samples were characterized in details. Different techniques were used: x-ray powder diffraction analysis, Raman spectral analysis, elemental analysis, and determination of textural and morphological properties. Obtained results showed ...
    ... LiOH) by hydrothermal treatment (HTC) treatment. After preparation, samples were characterized in details. Different techniques were used: x-ray powder diffraction analysis, Raman spectral analysis, elemental analysis, and determination of textural and morphological properties. Obtained results showed ...
    ... and KOH activated fructose, respectively. 2.2. Characterization Methods The crystal structure of the obtained samples was characterized by x-ray powder diffraction (XRPD) analysis using Ultima IV Rigaku diffractometer (Rigaku, The Woodlands, TX, USA), equipped with Cu Kα 1,2 radiation source (a generator ...

  • Structural characterization of traditional pottery produced from local clay, Rujište (Ražanj, Central Serbia), in an effort to preserve its geoheritage

    Maja Milošević, Biljana Đorđević, Alena Zdravković (2021)
    ... vessel walls. In order to confirm the presence and closer determination of individual minerals from the group of clays, oriented preparations (X-ray diffraction) were made. Studies conducted with a scanning electron microscope (SEM) equipped with a detector for secondary electrons (SE), back-scattered ...
    ... ratio of coarse-grained particles and the fine-grained fraction in the basic mass. Microcrystalline clasts could not be accurately identified. An X-ray powder diagram of the sample and database search revealed that the following minerals mailto:maja.milosevic@rgf.bg.ac.rs mailto:alena.zdravkovic@rgf ...

  • Influence of Ag doping on the morphological and magnetic properties in CuO nanopowders

    Maria Čebela, Uroš Čakar, Vesna Lojpur, Maja Milošević, Sanja Krstić, Vladimir Dodevski, Milena Rosić (2023)
    ... with the composition Cu,,Ag,O (x=0.01-0.05), a self- propagating synthesis was applied at room temperature, during which a successful reaction between metal nitrate and sodium hydroxide occurred. Prepared powders were calcinated at 700 "C for 2 h. The diffraction pattern was recorded at room ...