Претрага
136 items
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Structural dissymmetrization of optically anisotropic Grs64±1Adr36±1Sps2 grandite from Meka Presedla (Kopaonik Mt., Serbia)
In this paper, grandite core with Grs64±1Adr36±1Sps2composition was crystallographically studied. This core represents zone A of the macroscopically visiblefive A–E zones of the optically anisotropic Grs58–64 Adr36–42Sps2 grandite. The applied procedure includes the detailed analysis of the powder diffraction patterns, and the Rietveld refinements of the crystal structures in a series of 18 space groups and two mixtures, which were followed by the comparative analysis of the R-values, site occupancy factors, and the bond lengths and angles. Synthesis of all ...Pavle Tančić, Aleksandar Kremenović, Predrag Vulić. "Structural dissymmetrization of optically anisotropic Grs64±1Adr36±1Sps2 grandite from Meka Presedla (Kopaonik Mt., Serbia)" in Powder Diffraction, Cambridge University Press (CUP) (2019). https://doi.org/10.1017/S0885715619000897 М23
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Crystallography and Surface Oxidation of Stoichiometric Arsenopyrite from Šumadija-Kopaonik Pb-Zn/Polymetallic Ore District (Serbia)
Ivana Jelić, Aleksandar Pačevski, Aleksandar Kremenović, Aleš Šoster, Andreja Šestan, Janez Zavašnik (2023)The behaviour and stability of arsenopyrite largely depend on its crystal structure, but studies of crystallography and structural defects are scarce. For clarification, we investigated a series of natural arsenopyrite crystals from the polymetallic Pb-Zn-(±Cu,Ag,Au,Sb,Bi,W) Šumadija-Kopaonik ore district (Serbia) by powder X-ray diffraction (XRPD). Among them, samples from the Drenjak gold mineralisation showed near-stoichiometric FeAsS composition and were further investigated by conventional and high-resolution transmission electron microscopy methods. TEM revealed abundant planar crystallographic defects and epitaxial surface oxide layer ...Inorganic Chemistry, Condensed Matter Physics,General Materials Science, General Chemical Engineering, crystal structure, FeAsS, oxidation, TEM, XRPDIvana Jelić, Aleksandar Pačevski, Aleksandar Kremenović, Aleš Šoster, Andreja Šestan, Janez Zavašnik. "Crystallography and Surface Oxidation of Stoichiometric Arsenopyrite from Šumadija-Kopaonik Pb-Zn/Polymetallic Ore District (Serbia)" in Crystals, MDPI AG (2023). https://doi.org/10.3390/cryst13020278 М22
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A new copper(II) arsenate, Na2Cu3(AsO3OH)4·4H2O containing discrete [Cu3O12]18− units: Synthesis, crystal structure and magnetic properties
Single crystals of the new disodium tricopper(II) tetrakis(hydrogenarsenate(V)) tetrahydrate, Na2Cu3(AsO3OH)4·4H2O were grown under hydrothermal conditions. The compound was characterized by room-temperature single-crystal X-ray diffraction, SEM-EDS analysis, Raman spectroscopy and magnetic susceptibility measurements. Na2Cu3(AsO3OH)4·4H2O represents a new layered structure-type [space group P21/c, a = 8.7089(17), b = 9.7452(19), c = 9.3353(19) Å, β = 92.63(3)°, V = 791.4(3) Å3, Z = 4]. The layers are normal to [100] and are composed of the isolated Cu3O12 units interconnected by AsO3OH coordination ...Na2Cu3(AsO3OH)4•4H2O, хидротермална синтеза, кристална структура, хидрирани хидрокси-арсенати, магнетна својстваTamara Đorđević, Ljiljana Karanović, Zvonko Jagličić. "A new copper(II) arsenate, Na2Cu3(AsO3OH)4·4H2O containing discrete [Cu3O12]18− units: Synthesis, crystal structure and magnetic properties" in Journal of Solid State Chemistry, Elsevier BV (2018). https://doi.org/10.1016/j.jssc.2018.05.024 М22
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Sinteza i strukturna karakterizacija novih cezijumskih i kalijumskih silikata sa elementima retkih zemalja
Predrag Z. Dabić (2022)Predmet i ciljevi naučnog istraživanja ove doktorske disertacije su sinteza i strukturna karakterizacija novih cezijumskih i kalijumskih silikata sa elementima retkih zemalja. Istraživanja su izvedena u okviru sistema SiO2–REE2O3–XF, gde REE predstavlja trovalentni katjon elementa retkih zemalja (Sc, Y, Sm, Eu, Gd, Ho, Er, Tm, Yb, Lu), dok X predstavlja jednovalentni katjon alkalnih metala (K, Cs). Rad na disertaciji bio je fokusiran na sintezu monokristala, određivanje kristalnih struktura, kao i na kristalografsko i kristalohemijsko ispitivanje sintetisanih monokristala. Monokristali su sintetisani ...alkalni silikati elemenata retkih zemalja, kristalna struktura, sinteza metodom fluksa, rendgenska difrakcija na monokristalu, elementi retkih zemaljaPredrag Z. Dabić. Sinteza i strukturna karakterizacija novih cezijumskih i kalijumskih silikata sa elementima retkih zemalja, Beograd : P. Dabić, 2022 M70
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From mixed brookite/anatase TiO2 nanopowder to sodium titanates: Insight into morphology, structure, and photocatalytic performance
Nataša Tomić, Mirjana Grujić-Brojčin, Aleksandar Kremenović, Mirjana Novaković, Vladimir Lazović, Maja Šćepanović (2024)A method to obtain sodium titanate nanoribbons starting from a mixture of brookite and anatase TiO₂ nanopowder is described. As-prepared TiO2 nanopowder with a major brookite phase was used as a precursor in an alkaline hydrothermal approach, where the temperature was kept at 200 °C. The influence of hydrothermal treatment and consequent annealing temperature (T = 500 ) on the crystal structure, phase composition, and morphology of samples were investigated by X-ray powder diffraction (XRPD), Raman and FTIR spectroscopy, ...nanostrukturirani materijali, hemijska sinteza, difrakcija rendgenskih zraka, skenirajuća elektronska mikroskopija, kristalna struktura, katalizaNataša Tomić, Mirjana Grujić-Brojčin, Aleksandar Kremenović, Mirjana Novaković, Vladimir Lazović, Maja Šćepanović. "From mixed brookite/anatase TiO2 nanopowder to sodium titanates: Insight into morphology, structure, and photocatalytic performance" in Ceramics International, Elsevier BV (2024). https://doi.org/10.1016/j.ceramint.2024.10.063 М21
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A new polymorph of Ba(AsO3OH): Synthesis, crystal structure and vibrational spectra
Tamara Đorđević, Ljiljana Karanović (2010)A new monoclinic polymorph of Ba(AsO3OH) was synthesized under hydrothermal conditions. It represents a previously unknown structure type. Its crystal structure was determined from a racemic twin using single-crystal X-ray diffraction data collected at 120 and 293 K [space group P21, a=7.2149(14)/7.2370(2), b=7.7028(15)/7.7133(2), c=21.7385(43)/21.8079(5) Å, β=95.95(3)/96.073(1)1, V=1201.6(4)/1210.51(5) Å3, Z=12]. The crystal structure of P21-Ba(AsO3OH) has a layered character and is built up of four types of regularly alternating layers parallel to (0 0 1). Every AsO3OH tetrahedron is chelating to two Ba atoms and ...Ba(AsO3OH), хидротермална синтеза, структурна анализа монокристала, Раманска спектроскопија, инфрацрвена спектроскопија, водоничне везе, хидрогенарсенати земноалкалних металаTamara Đorđević, Ljiljana Karanović. "A new polymorph of Ba(AsO3OH): Synthesis, crystal structure and vibrational spectra" in Journal of Solid State Chemistry, Elsevier BV (2010). https://doi.org/10.1016/j.jssc.2010.09.027 М22
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Water in the Alluaudite Type-Compounds: Synthesis, Crystal Structure and Magnetic Properties of Co3(AsO4)0.5+x(HAsO4)2−x(H2AsO4)0.5+x[(H,□)0.5(H2O,H3O)0.5]2x+
In this study, a new cobalt arsenate belonging to the alluaudite supergroup compounds with the general formula of Co3(AsO4)0.5+x(HAsO4)2−x(H2AsO4)0.5+x[(H, )0.5(H2O,H3O)0.5]2x+ (denoted as CoAsAllu) was synthesized under hydrothermal conditions. Its crystal structure was determined by a room-temperature single-crystal X-ray diffraction analysis: space group C2/c, a = 11.6978(8), b = 12.5713(7), c = 6.7705(5) Å, b = 113.255(5)◦, V = 914.76(11) Å3, Z = 2 for As6H8Co6O25. It represents a new member of alluaudite-like protonated arsenates and the first alluaudite-like phase ...супергрупа алуаудита, арсенати прелазних метала, хидротермална синтеза, кристална структура, хидратисани хидрокси-арсенати, стехиометрија, магнетна својстваTamara Đorđević, Ljiljana Karanović, Marko Jagodič, Zvonko Jagličić. "Water in the Alluaudite Type-Compounds: Synthesis, Crystal Structure and Magnetic Properties of Co3(AsO4)0.5+x(HAsO4)2−x(H2AsO4)0.5+x[(H,□)0.5(H2O,H3O)0.5]2x+" in Minerals, MDPI AG (2021). https://doi.org/10.3390/min11121372 М22
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Three new Sr-bearing arsenates, hydrothermally synthesized in the system SrO–MO–As2O5–H2O (M2+ = Mg, Cu, Zn)
Tamara Đorđević, Ljiljana Karanović (2018)During systematic research on the mineral-related synthetic arsenates, with particular focus on their structural and spectroscopic classification, three new Sr-containing arsenates Sr2Mg(AsO4)2· 2H2O (1), Sr2Zn4(AsO4)4·H2O (2) and Sr2Cu7(AsO4)6 (3) have been synthesized under low-temperature hydrothermal conditions in the system SrO MO As2O5 H2O (M 2þ = Mg, Zn, Cu). Their crystal structures were determined using room-temperature single-crystal X-ray diffraction data and refined to the following R-values: 1– R1 = 0.025; 2– R1 = 0.030; 3– R1 = 0.035. Compounds ...стронцијум, арсен, арсенати, кристална структура, дифракција рендгенских зрака на монокристалима, хидротермална синтеза, Раманска спектроскопијаTamara Đorđević, Ljiljana Karanović. "Three new Sr-bearing arsenates, hydrothermally synthesized in the system SrO–MO–As2O5–H2O (M2+ = Mg, Cu, Zn)" in European Journal of Mineralogy, Schweizerbart (2018). https://doi.org/10.1127/ejm/2018/0030-2749 М22
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Ionothermal synthesis and crystal structure of a new organic–inorganic hybrid compound:catena-poly[bis(1-ethyl-3-methylimidazolium) [hepta-μ-bromido-pentacuprate(I)]]
A new organic-inorganic hybrid compound, catena-poly[bis(1-ethyl-3-methylimidazolium) [μ5-bromido-tri-μ3-bromido-tri-μ2-bromido-pentacuprate(I)]], {(C6H11N2)2[Cu5Br7]}n, has been obtained under ionothermal conditions from a reaction mixture containing Ba(OH)2•8H O, Cu(OH)2•2H2O, As2O5 , 1-ethyl-3-methylimidazolium bromide and distilled water. The crystal structure consists of complex [Cu5Br7]2- anions arranged in sinusoidal {[Cu5Br7]2-}n chains running along the a axis, which are surrounded by 1-ethyl-3-methylimidazolium cations. Three of the five unique Br atoms and one of the three Cu(I) atoms occupy special positions with half-occupancy (a mirror plane perpendicular to the b ...кристална структура, органско-неорганско хибридно једињење, бакар(I) бромид, јонотермна синтеза, 1-етил-3-метилимидазолијум бромид, Cu•••Cu интеракцијеLjiljana Karanović, Dejan Poleti, Tamara Đorđević. "Ionothermal synthesis and crystal structure of a new organic–inorganic hybrid compound:catena-poly[bis(1-ethyl-3-methylimidazolium) [hepta-μ-bromido-pentacuprate(I)]]" in Acta Crystallographica Section C Structural Chemistry, International Union of Crystallography (IUCr) (2014). https://doi.org/10.1107/S205322961402172X М23
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Synthesis, magnetic, thermal and structural properties of Co(II), Ni(II) and Cu(II) complexes containing isophthalato ligands
A series of novel ternary Co(II), Ni(II) and Cu(II) complexes containing 2,20-dipyridylamine (dipya), 2,20-bipyridine (bipy), and 1,10-phenanthroline (phen), as aromatic diamine ligands, and dianion of isophthalic acid (ipht) have been prepared by ligand exchange reactions from diluted H2O/EtOH solutions. The complexes were characterized by elemental analysis, IR spectroscopy, magnetic susceptibility measurements and TG and DSC analysis. Three complexes, Cu(dipya)(ipht)H2O (1), Co(dipya)(ipht)2H2O (2) and Cu(ipht)(phen)2H2O (5) are polymeric with bis-monodentate ipht, while the other two complexes M(bipy)(ipht)4H2O, M@Co(II) (3) and ...комплекси прелазних метала, карбоксилатни лиганди, N-лиганди, кристална структура, магнетна својстваJelena Rogan, Dejan Poleti, Ljiljana Karanović, Zvonko Jagličić. "Synthesis, magnetic, thermal and structural properties of Co(II), Ni(II) and Cu(II) complexes containing isophthalato ligands" in Journal of Molecular Structure, Elsevier BV (2011). https://doi.org/10.1016/j.molstruc.2010.11.024 М23
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The role of non-covalent intermolecular interactions on the diversity of crystal packing in supramolecular dihalopyridine–silver(i) nitrate complexes
Sunčica Roca, Lucija Hok, Robert Vianello, Mladen Borovina, Marijana Đaković, Ljiljana Karanović, Dražen Vikić-Topić, Zora Popović (2020)Six novel 1 : 2 complexes of silver(I) nitrate with 2,5-, 2,6- and 3,5-dihalopyridines (halo stands for chlorine and bromine) were prepared by the reaction of an aqueous solution of AgNO3 and the corresponding pyridine derivative in a water–alcohol solution. In spite of having analogous empirical formulae, they reveal intriguing structural differences, except [Ag(NO3)(2,5-Cl2py)2]n (1) and [Ag(NO3)(2,5-Br2py)2]n (4), which are isostructural. In contrast, [Ag(NO3)(3,5-Cl2py)2]2 (3) is dimeric, while its Br analogue [Ag(NO3)(3,5-Br2py)2]n (6) is polymeric in nature, being the ...Sunčica Roca, Lucija Hok, Robert Vianello, Mladen Borovina, Marijana Đaković, Ljiljana Karanović, Dražen Vikić-Topić, Zora Popović. "The role of non-covalent intermolecular interactions on the diversity of crystal packing in supramolecular dihalopyridine–silver(i) nitrate complexes" in CrystEngComm, Royal Society of Chemistry (RSC) (2020). https://doi.org/10.1039/D0CE01257B М22
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Crystal Structure and Chemical Composition of Ludwigite from Vranovac Ore deposit (Boranja Mountain, Serbia)
Tančić Pavle, Dimitrijević Radovan, Poznanović Maja, Pačevski Aleksandar, Sudar Slobodanka. "Crystal Structure and Chemical Composition of Ludwigite from Vranovac Ore deposit (Boranja Mountain, Serbia)" in Acta Geologica Sinica 86, Beijing:Geological Society of China (2012): 1524-1538 M22
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Crystal-chemistry of the alkaline-earth hydrogen arsenates: crystal structure and vibrational spectraof a new Ba(AsO3OH) polymorphic variety
Đorđević Tamara, Karanović Ljiljana (2010)Đorđević Tamara, Karanović Ljiljana. "Crystal-chemistry of the alkaline-earth hydrogen arsenates: crystal structure and vibrational spectraof a new Ba(AsO3OH) polymorphic variety" in Book of Abstracts, XI General Meeting of the Russian Mineralogical Society combined with Fedorov Session, St. Petersburg, Russia: (2010): 88-89 M34
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Crystal structure of Ba[Co3(OH)2(VO4)2] - Кристална структура Ba[Co3(OH)2(VO4)2]
Đorđević Tamara, Karanović Ljiljana (2011)Đorđević Tamara, Karanović Ljiljana. "Crystal structure of Ba[Co3(OH)2(VO4)2] - Кристална структура Ba[Co3(OH)2(VO4)2]" in XVIII Konferencija Srpskog kristalografskog društva, Izvodi radova, Andrevlje, Srbija:Srpsko kristalografsko društvo (2011): 60-61 M64
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Crystal structure of Cd5(VO4)2(OH)4 and CdV3O7 - Кристалне структуре Cd5(VO4)2(OH)4 и CdV3O7.
Đorđević Tamara, Karanović Ljiljana (2013)Đorđević Tamara, Karanović Ljiljana. "Crystal structure of Cd5(VO4)2(OH)4 and CdV3O7 - Кристалне структуре Cd5(VO4)2(OH)4 и CdV3O7." in XX Konferencija Srpskog kristalografskog društva, Izvodi radova, Avala, Srbija:Srpsko kristalografsko društvo (2013): 64-65 M64
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Defect detection in aluminium using pulse thermography for sample width periodic structure
Damnjanović Vesna, Goran Dikić, B. Milanović and Slobodan Petričević. "Defect detection in aluminium using pulse thermography for sample width periodic structure" in FOTONIKA 2017, VI International School and Conference on Photonics, Beograd, Srbija:Institute of Physics Belgrade (2017): 82 M34
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Geology of the Čoka structure in northern Banat (Central Paratethys, Serbia)
Radivojević Dеjan, Rundić Lјupko, Knežević Slobodan. "Geology of the Čoka structure in northern Banat (Central Paratethys, Serbia)" in Geologica Carpathica 4 no. 61, Bratislava, Slovačka:Geological Institute of the Slovak Academy of Sciences (2010): 341-352 M23
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Shallow-landslide spatial structure interpretation using a multi-geophysical approach
Ristić Aleksandar, Abolmasov Biljana, Govedarica Miro, Petrovački Dušan, Ristić Aleksandra. "Shallow-landslide spatial structure interpretation using a multi-geophysical approach" in Acta Geotechnica Slovenica 9 no. 1, Ljubljana, Slovenia:University of Maribor, University of Ljubljana, Slovenian Geotechnical Society (2012): 47-59 M23
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Energy geo-structure for sustainable development
Rakić Dragoslav, Basarić Irena (2014)Rakić Dragoslav, Basarić Irena. "Energy geo-structure for sustainable development" in Zbornik radova = Proceedings / 9. simpozijum Reciklažne tehnologije i održivi razvoj sa međunarodnim učešćem, Zaječar, 10.-12. septembar 2014. godine = 9th Symposium Recycling Technologies and Sustainable Development with International Participat 9, Zaječar, Srbija:Univerzitet u Beogradu Tehnički fakultet u Boru (2014): 476-481 M33
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Crystal structure of the body-centered tetragonal tectosilicate K1.13Al1.13Si0.87O4
Vulić Predrag, Lazić Biljana, Kremenović Aleksandar. "Crystal structure of the body-centered tetragonal tectosilicate K1.13Al1.13Si0.87O4" in XX Conference of the Serbian Crystallographic Society-Abstracts, Avala, Beograd, Srbija:Srpsko kristalografsko društvo (2013): 54-55 M64